Institute of Chemical Research of Catalonia (ICIQ), The Barcelona Institute of Science and Technology, Av. Països Catalans 16, 43007 Tarragona, Spain ...
Interestingly, we found that the readily accessible aryl vinyl 1,3-diol, an intermediate en route to the synthesis of oxetane, is an equally potential precursor for the anticipated cyclization.
Our methods consists of dissolving a diol in a mineral acid, introducing the mixture into a heated solution of base, and distilling off the cyclic ether produced.
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