Figure 1: Schematic diagram of the magic-angle coil spinning (MACS) insert. In solid-state NMR experiments, the size of the anisotropic interactions is usually of the same order of magnitude or ...

Step 1 starts with the sample inside the NMR magnet. Figure 1: Schematic representation of the (H)NH correlation experiment pulse sequence. Set the duration of the 180° XY decoupling pulses ...